UID:
almahu_9948026138402882
Format:
1 online resource (1151 p.)
Edition:
1st ed.
ISBN:
1-281-79587-9
,
9786611795870
,
0-08-054069-4
Series Statement:
Techniques and instrumentation in analytical chemistry ; v. 21
Uniform Title:
Environmental analysis (Amsterdam, Netherlands)
Content:
This book is an updated, completely revised version of a previous volume in this series entitled: ENVIRONMENTAL ANALYSIS -- Techniques, applications and quality assurance. The book treats different aspects of environmental analysis such as sample handling and analytical techniques, the applications to trace analysis of pollutants (mainly organic compounds), and quality assurance aspects, including the use of certified reference materials for the quality control of the whole analytical process. New analytical techniques are presented that have been developed significantly over the last 6 years,
Note:
"This book is an updated, completely revised version of a previous volume in this series entitled: Environmental analysis--techniques and quality assurance"--Pref.
,
Front Cover; Sample Handling and Trace Analysis of Pollutants: Techniques, Applications and Quality Assurance; Copyright Page; CONTENTS; Preface; PART I: FIELD SAMPLING TECHNIQUES AND SAMPLE PREPARATION; CHAPTER 1. SAMPLE HANDLING STRATEGIES FOR THE ANALYSIS OF ORGANIC COMPOUNDS IN ENVIRONMENTAL WATER SAMPLES; 1.1 Introduction; 1.2 Liquid-liquid extraction procedures; 1.3 Supported liquid membrane extraction procedures; 1.4 Solid-phase extraction; 1.5 Clean-up of samples; 1.6 On-line coupling of SPE to LC; 1.7 Conclusion and further developments; References
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CHAPTER 2. SEPARATION, CLEAN-UP AND RECOVERIES OF PERSISTENT TRACE ORGANIC CONTAMINANTS FROM SOILS, SEDIMENT AND BIOLOGICAL MATRICES2.1 Introduction; 2.2 Sample preservation and storage; 2.3 Recoveries; 2.4 Extraction; 2.5 Clean-up and group separation; 2.6 Group separation and multi-residue schemes; 2.7 Confirmatory methods; 2.8 Quality assurance and interlaboratory studies; 2.9 Hyphenated techniques; 2.10 Health and safety; References; CHAPTER 3. APPLICATIONS OF MICROWAVE-ASSISTED EXTRACTION IN ENVIRONMENTAL ANALYSIS; 3.1 Sample preparation techniques in environmental analysis
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3.2 Fundamentals of MAE3.3 Instrumentation; 3.4 Applications of microwave-assisted extraction; 3.5 Future directions; References; CHAPTER 4. SAMPLE HANDLING AND ANALYSIS OF PESTICIDES AND THEIR TRANSFORMATION PRODUCTS IN WATER MATRICES BY LIQUID CHROMATOGRAPHIC TECHNIQUES; 4.1 Introduction; 4.2 Sample handling (extraction and clean-up); 4.3 LC determination of pesticides (except MS detection); 4.4 LC-MS; 4.5 Conclusions; Acknowledgements; References; PART II: APPLICATION AREAS; CHAPTER 5. ENVIRONMENTAL APPLICATIONS OF GAS CHROMATOGRAPHY-ATOMIC EMISSION DETECTION; 5.1 Introduction
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5.2 Instrumentation5.3 Applications; 5.4 Conclusion; References; CHAPTER 6. METHODS FOR THE DETERMINATION AND EVALUATION OF CHLORINATED BIPHENYLS (CBs) IN ENVIRONMENTAL MATRICES; 6.1 Introduction; 6.2 Sources of PCBs; 6.3 Compound selection; 6.4 Matrix extraction; 6.5 Clean-up; 6.6 Group separation; 6.7 LC-GC combinations; 6.8 Analytical chromatography; 6.9 Detection; 6.10 Quality assurance; 6.11 Data interpretation; References; CHAPTER 7. IMMUNOASSAYS FOR ENVIRONMENTAL ANALYSIS; 7.1 Introduction; 7.2 Types of immunoassays; 7.3 Antibodies; 7.4 Hapten design
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7.5 Conjugation procedures using proteins or enzymes7.6. Immunoassay features; 7.7 Matrix effect; 7.8 Validation studies; 7.9 Conclusions and future developments; Acknowledgements; References; CHAPTER 8. COUPLED-COLUMN LC (LC/LC) IN ENVIRONMENTAL TRACE ANALYSIS OF POLAR PESTICIDES; 8.1 Introduction; 8.2 Coupled-column liquid chromatography (LC/LC); 8.3 LC/LC-UV; 8.4 LC/LC with selective detection; 8.5 Systematic method-development; 8.6 Conclusions; Acknowledgements; References
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CHAPTER 9. LIQUID CHROMATOGRAPHIC AND BIORECOGNITION TECHNIQUES FOR THE DETERMINATION OF PHENOLS AND THEIR SUBSTITUTED DERIVATIVES IN WATER SAMPLES
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English
Additional Edition:
ISBN 0-444-82831-1
Language:
English
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