UID:
almafu_9958132833802883
Format:
1 online resource (353 p.)
ISBN:
0-444-59907-X
Series Statement:
Analytical spectroscopy library ; v. 3
Content:
Today, atomic emission spectroscopy is a well-established analytical technique of widespread application - a technique that no-one involved or interested in chemical analysis can afford to ignore. The present book was written to meet the need for an extensive introduction to this technique. It is written in an easy-to-understand way, and is mainly aimed at tertiary-level students at universities and colleges, and at newcomers to the field.The book prepares the reader for the study of more advanced texts and the increasing number of research papers published in this area. It will not on
Note:
Description based upon print version of record.
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Front Cover; Introduction to Inductively Coupled Plasma Atomic Emission Spectrometry; Copyright Page; Table of Contents; Foreword; Preface; CHAPTER 1. PRINCIPLES AND HISTORY OF ATOMIC EMISSION SPECTROSCOPY; 1.1 Introduction; 1.2 Principles of atomic emission spectroscopy; 1.3 History; 1.4 Information sources; References; CHAPTER 2. SPECTROGRAPHIC ANALYSIS; 2.1 Introduction; 2.2 Spectrographic equipment; 2.3 Spectra; 2.4 Problems in spectrographic analysis; 2.5 Spectrography and spectrometry; References; CHAPTER 3. EXCITATION SOURCES; 3.1 Introduction; 3.2 Direct current arc
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3.3 Gas-stabilized d.c. arc3.4 Plasma jet; 3.5 Three-electrode direct current plasma; 3.6 Spark discharge; 3.7 Hollow cathode lamp; 3.8 Glow discharge lamp; 3.9 Microwave plasmas; 3.10 Lasers; 3.11 Inductively coupled plasma; 3.12 Summary; References; CHAPTER 4. INDUCTIVELY COUPLED PLASMAS; 4.1 Introduction and history; 4.2 ICP formation; 4.3 ICP mechanisms; 4.4 ICP torches; References; CHAPTER 5. INSTRUMENTATION; 5.1 Introduction; 5.2 Radiofrequency oscillators; 5.3 Spectrometers; 5.4 Conclusion; References; CHAPTER 6. INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY
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6.1 ICP nomenclature6.2 Analytical application of an ICP; 6.3 Comparison of techniques; 6.4 Low gas flow ICP-AES; 6.5 Mixed gas ICPs; 6.6 Organic solvents; 6.7 Side-on or end-on plasma viewing; 6.8 Laminar flow ICP; 6.9 Extended ICP torch; 6.10 High-pressure ICP; 6.11 Purchasing an ICP-AES system; References; CHAPTER 7. NEBULIZATION; 7.1 Introduction; 7.2 Theory of nebulizers; 7.3 Nebulizers; 7.4 Conclusion; References; CHAPTER 8. SAMPLE DISSOLUTION; 8.1 Introduction; 8.2 Dissolution of samples for multi-element analysis; 8.3 Treatment of organic materials; 8.4 Treatment of liquid samples
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8.5 Dissolution of solid samples8.6 Dissolution of geological materials; 8.7 Dissolution of samples containing boron; 8.8 Conclusion; References; CHAPTER 9. SAMPLE INTRODUCTION; 9.1 Introduction; 9.2 Introduction of gases; 9.3 Introduction of liquids; 9.4 Introduction of solids; 9.5 Automation; 9.6 Conclusion; References; CHAPTER 10. ANALYSIS; 10.1 Introduction; 10.2 Analysis by ICP-AES; 10.3 Calibration; 10.4 Figures of merit; 10.5 Analytical applications; 10.6 Everyday operation; 10.7 Conclusion and future trends; References; CHAPTER 11. ACCURACY AND PRECISION; 11.1 Introduction
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11.2 The meaning of accuracy and precision11.3 Errors; 11.4 The measurement of accuracy and precision; 11.5 Reproducibility and repeatability; 11.6 Reference materials; 11.7 Confidence limits; 11.8 Factors affecting accuracy and precision; 11.9 Statistics; 11.10 Background equivalent concentration; 11.11 Improving accuracy and precision; 11.12 Conclusion; References; CHAPTER 12. INTERNAL STANDARDIZATION; 12.1 Introduction; 12.2 Basic principles of internal standardization; 12.3 Improvement in precision with i.s; 12.4 The effect of variation in plasma parameters
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12.5 The effect of i.s. on routine operation and concentration results
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English
Additional Edition:
ISBN 0-444-43029-6
Language:
English
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