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  • 1
    Book
    Book
    Membrane reactors : distributing reactants to improve selectivity and yield (2010)
    Weinheim :Wiley-VCH,
    Details
    UID:
    almahu_BV036073894
    Format: XVIII, 274 S. : , Ill., graph. Darst.
    ISBN: 978-3-527-32039-4
    Language: English
    Subjects: Chemistry/Pharmacy
    RVK:
    VE 7100
    RVK:
    VN 7320
    Keywords: Membranreaktor ; Aufsatzsammlung ; Fallstudiensammlung
    URL: Inhaltstext
    URL: Inhaltsverzeichnis
    Author information: Seidel-Morgenstern, Andreas 1956-
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  • 2
    Book
    Book
    Membrane reactors : distributing reactants to improve selectivity and yield (2010)
    Weinheim : Wiley-VCH
    Details
    UID:
    b3kat_BV036073894
    Format: XVIII, 274 S. , Ill., graph. Darst.
    ISBN: 9783527320394
    Language: English
    Subjects: Chemistry/Pharmacy
    RVK:
    VE 7100
    RVK:
    VN 7320
    Keywords: Membranreaktor ; Aufsatzsammlung ; Fallstudiensammlung
    URL: Inhaltstext
    URL: Inhaltsverzeichnis
    Author information: Seidel-Morgenstern, Andreas 1956-
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  • 3
    Online Resource
    Online Resource
    Integrated chemical processes : synthesis, operation, analysis, and control (2005)
    Weinheim :Wiley-VCH,
    Details
    UID:
    almafu_9959328721002883
    Format: 1 online resource (xxvi, 540 pages) : , illustrations
    Edition: Electronic reproduction. [Place of publication not identified] : HathiTrust Digital Library, 2010.
    ISBN: 352760555X , 9783527605552 , 3527308318 , 9783527308316 , 3527605738 , 9783527605736 , 1280520612 , 9781280520617
    Content: This is the first book dedicated to the entire field of integrated chemical processes, covering process design, analysis, operation and control of these processes. Both the editors and authors are internationally recognized experts from different fields in industry and academia, and their contributions describe all aspects of intelligent integrations of chemical reactions and physical unit operations such as heat exchange, separational operations and mechanical unit operations. As a unique feature, the book also introduces new concepts for treating different integration concepts on a generaliz.
    Note: PART I. INTEGRATION OF HEAT TRANSFER AND CHEMICAL REACTIONS -- , Enhancing productivity and thermal efficiencey of high-temperature endothermic processes in heat-integrated fixed-bed reactors / , Conceptual design of internal reforming in high-temperature fuel cells / , Instabilities in high-temperature fuel cells due to combined heat and charge transport / , PART II. INTEGRATION OF SEPARATIONS AND CHEMICAL REACTIONS -- , Thermodynamic and kinetic effects on the feasible products of reactive distillation: a-zeo-tropes and a-rheo-tropes / , Equilibrium theory and nonlinear waves for reaction separation processes / , Simulated moving-bed reactors / , The dos and don'ts of adsorptive reactors / , Reactive stripping in structured catalytic reactors: hydrodynamics and reaction performance / , Reactive absorption / , Reactive extraction: principles and apparatus concepts / , Development of reactive crystallization processes / , Analysis and experimental investigation of catalytic membrane reactors / , PART III. INTEGRATION OF MECHANICAL OPERATIONS AND CHEMICAL REACTIONS -- , Reactive extrusion for solvent-free processing: facts and fantasies / , Reactive comminution / , Reactive filtration / , Reaction-assisted granulation in fluidized beds / , Master and use copy. Digital master created according to Benchmark for Faithful Digital Reproductions of Monographs and Serials, Version 1. Digital Library Federation, December 2002.
    Additional Edition: Print version: Integrated chemical processes. Weinheim : Wiley-VCH, ©2005 ISBN 3527308318
    Language: English
    Keywords: Electronic books. ; Electronic books. ; Electronic books.
    DOI: 10.1002/3527605738
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/3527605738
    URL: Volltext
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/3527605738
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/3527605738
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  • 4
    Online Resource
    Online Resource
    Preparative chromatography / (2020)
    Weinheim :Wiley-VCH,
    Details
    UID:
    almafu_9959359196902883
    Format: 1 online resource
    Edition: Third edition.
    ISBN: 9783527816330 , 352781633X , 9783527816347 , 3527816348
    Note: 〈p〉Preface xv〈/p〉 〈p〉About the Editors xvii〈/p〉 〈p〉List of Abbreviations xix〈/p〉 〈p〉Notation xxiii〈/p〉 〈p〉〈b〉1 Introduction 〈/b〉〈b〉1〈br /〉〈/b〉〈i〉Henner Schmidt-Traub and Reinhard Ditz〈/i〉〈/p〉 〈p〉1.1 Chromatography, Development, and Future Trends 1〈/p〉 〈p〉1.2 Focus of the Book 4〈/p〉 〈p〉1.3 Suggestions on How to Read this Book 4〈/p〉 〈p〉References 6〈/p〉 〈p〉〈b〉2 Fundamentals and General Terminology 〈/b〉〈b〉9〈br /〉〈/b〉〈i〉Andreas Seidel-Morgenstern〈/i〉〈/p〉 〈p〉2.1 Principles and Features of Chromatography 9〈/p〉 〈p〉2.2 Analysis and Description of Chromatograms 13〈/p〉 〈p〉2.2.1 Voidage and Porosity 13〈/p〉 〈p〉2.2.2 Retention Times and Capacity Factors 16〈/p〉 〈p〉2.2.3 Efficiency of Chromatographic Separations 17〈/p〉 〈p〉2.2.4 Resolution 20〈/p〉 〈p〉2.2.5 Pressure Drop 23〈/p〉 〈p〉2.3 Mass Transfer and Fluid Dynamics 25〈/p〉 〈p〉2.3.1 Principles of Mass Transfer 25〈/p〉 〈p〉2.3.2 Fluid Distribution in the Column 27〈/p〉 〈p〉2.3.3 Packing Nonidealities 28〈/p〉 〈p〉2.3.4 Extra-Column Effects 29〈/p〉 〈p〉2.4 Equilibrium Thermodynamics 29〈/p〉 〈p〉2.4.1 Definition of Isotherms 29〈/p〉 〈p〉2.4.2 Models of Isotherms 31〈/p〉 〈p〉2.4.2.1 Single-Component Isotherms 31〈/p〉 〈p〉2.4.2.2 Multicomponent Isotherms Based on the Langmuir Model 33〈/p〉 〈p〉2.4.2.3 Competitive Isotherms Based on the Ideal Adsorbed Solution Theory 34〈/p〉 〈p〉2.4.2.4 Steric Mass Action Isotherms 37〈/p〉 〈p〉2.4.3 Relation Between Isotherms and Band Shapes 38〈/p〉 〈p〉2.5 Column Overloading and Operating Modes 44〈/p〉 〈p〉2.5.1 Overloading Strategies 44〈/p〉 〈p〉2.5.2 Beyond Isocratic Batch Elution 45〈/p〉 〈p〉References 46〈/p〉 〈p〉〈b〉3 Stationary Phases 〈/b〉〈b〉49〈br /〉〈/b〉〈i〉Michael Schulte〈/i〉〈/p〉 〈p〉3.1 Survey of Packings and Stationary Phases 49〈/p〉 〈p〉3.2 Inorganic Sorbents 50〈/p〉 〈p〉3.2.1 Activated Carbons 50〈/p〉 〈p〉3.2.2 Synthetic Zeolites 54〈/p〉 〈p〉3.2.3 Porous Oxides: Silica, Activated Alumina, Titania, Zirconia, and Magnesia 54〈/p〉 〈p〉3.2.4 Silica 55〈/p〉 〈p〉3.2.4.1 Surface Chemistry 57〈/p〉 〈p〉3.2.4.2 Mass Loadability 59〈/p〉 〈p〉3.2.5 Diatomaceous Earth 59〈/p〉 〈p〉3.2.6 Reversed Phase Silicas 60〈/p〉 〈p〉3.2.6.1 Silanization of the Silica Surface 60〈/p〉 〈p〉3.2.6.2 Silanization 60〈/p〉 〈p〉3.2.6.3 Starting Silanes 61〈/p〉 〈p〉3.2.6.4 Parent Porous Silica 61〈/p〉 〈p〉3.2.6.5 Reaction and Reaction Conditions 62〈/p〉 〈p〉3.2.6.6 Endcapping 62〈/p〉 〈p〉3.2.6.7 Chromatographic Characterization of Reversed Phase Silicas 63〈/p〉 〈p〉3.2.6.8 Chromatographic Performance 63〈/p〉 〈p〉3.2.6.9 Hydrophobic Properties Retention Factor (Amount of Organic Solvent for Elution), Selectivity 65〈/p〉 〈p〉3.2.6.10 Shape Selectivity 65〈/p〉 〈p〉3.2.6.11 Silanol Activity 67〈/p〉 〈p〉3.2.6.12 Purity 68〈/p〉 〈p〉3.2.6.13 Improved pH Stability Silica 68〈/p〉 〈p〉3.2.7 Aluminum Oxide 69〈/p〉 〈p〉3.2.8 Titanium Dioxide 70〈/p〉 〈p〉3.2.9 Other Oxides 71〈/p〉 〈p〉3.2.9.1 Magnesium Oxide 71〈/p〉 〈p〉3.2.9.2 Zirconium Dioxide 71〈/p〉 〈p〉3.2.10 Porous Glasses 72〈/p〉 〈p〉3.3 Cross-Linked Organic Polymers 73〈/p〉 〈p〉3.3.1 General Aspects 74〈/p〉 〈p〉3.3.2 Hydrophobic Polymer Stationary Phases 77〈/p〉 〈p〉3.3.3 Hydrophilic Polymer Stationary Phases 78〈/p〉 〈p〉3.3.4 Ion Exchange (IEX) 79〈/p〉 〈p〉3.3.4.1 Optimization of Ion-Exchange Resins 81〈/p〉 〈p〉3.3.5 Mixed Mode 88〈/p〉 〈p〉3.3.6 Hydroxyapatite 88〈/p〉 〈p〉3.3.7 Designed Adsorbents 91〈/p〉 〈p〉3.3.7.1 Protein A Affinity Sorbents 91〈/p〉 〈p〉3.3.7.2 Other IgG Receptor Proteins: Protein G and Protein L 96〈/p〉 〈p〉3.3.7.3 Sorbents for Derivatized/Tagged Compounds: Immobilized Metal Affinity Chromatography (IMAC) 96〈/p〉 〈p〉3.3.7.4 Other Tag-Based Affinity Sorbents 101〈/p〉 〈p〉3.3.8 Customized Adsorbents 102〈/p〉 〈p〉3.3.8.1 Low Molecular Weight Ligands 105〈/p〉 〈p〉3.3.8.2 Natural Polymers (Proteins, Polynucleotides) 108〈/p〉 〈p〉3.3.8.3 Artificial Polymers 111〈/p〉 〈p〉3.4 Advective Chromatographic Materials 111〈/p〉 〈p〉3.4.1 Adsorptive Membranes and Grafted-Polymer Membranes 114〈/p〉 〈p〉3.4.2 Adsorptive Nonwovens 115〈/p〉 〈p〉3.4.3 Fiber/Particle Composites 117〈/p〉 〈p〉3.4.4 Area-Enhanced Fibers 117〈/p〉 〈p〉3.4.5 Monolith 118〈/p〉 〈p〉3.4.6 Chromatographic Materials for Larger Molecules 121〈/p〉 〈p〉3.5 Chiral Stationary Phases 121〈/p〉 〈p〉3.5.1 Cellulose- and Amylose-Based CSP 122〈/p〉 〈p〉3.5.2 Antibiotic CSP 128〈/p〉 〈p〉3.5.3 Cyclofructan-Based CSP 128〈/p〉 〈p〉3.5.4 Synthetic Polymers 128〈/p〉 〈p〉3.5.5 Targeted Selector Design 130〈/p〉 〈p〉3.5.6 Further Developments 132〈/p〉 〈p〉3.6 Properties of Packings and Their Relevance to Chromatographic Performance 132〈/p〉 〈p〉3.6.1 Chemical and Physical Bulk Properties 132〈/p〉 〈p〉3.6.2 Morphology 133〈/p〉 〈p〉3.6.3 Particulate Adsorbents: Particle Size and Size Distribution 133〈/p〉 〈p〉3.6.4 Pore Texture 134〈/p〉 〈p〉3.6.5 Pore Structural Parameters 137〈/p〉 〈p〉3.6.6 Comparative Rating of Columns 137〈/p〉 〈p〉3.7 Sorbent Maintenance and Regeneration 138〈/p〉 〈p〉3.7.1 Cleaning in Place (CIP) 138〈/p〉 〈p〉3.7.2 CIP for IEX 140〈/p〉 〈p〉3.7.3 CIP of Protein A Sorbents 140〈/p〉 〈p〉3.7.4 Conditioning of Silica Surfaces 143〈/p〉 〈p〉3.7.5 Sanitization in Place (SIP) 145〈/p〉 〈p〉3.7.6 Column and Adsorbent Storage 145〈/p〉 〈p〉References 146〈/p〉 〈p〉〈b〉4 Selection of Chromatographic Systems 〈/b〉〈b〉159〈br /〉〈/b〉〈i〉Michael Schulte〈/i〉〈/p〉 〈p〉4.1 Definition of the Task 164〈/p〉 〈p〉4.2 Mobile Phases for Liquid Chromatography 167〈/p〉 〈p〉4.2.1 Stability 168〈/p〉 〈p〉4.2.2 Safety Concerns 172〈/p〉 〈p〉4.2.3 Operating Conditions 172〈/p〉 〈p〉4.2.4 Aqueous Buffer Systems 176〈/p〉 〈p〉4.3 Adsorbent and Phase Systems 178〈/p〉 〈p〉4.3.1 Choice of Phase System Dependent on Solubility 178〈/p〉 〈p〉4.3.2 Improving Loadability for Poor Solubilities 180〈/p〉 〈p〉4.3.3 Dependency of Solubility on Sample Purity 183〈/p〉 〈p〉4.3.4 Generic Gradients for Fast Separations 184〈/p〉 〈p〉4.4 Criteria for Choosing Normal Phase Systems 184〈/p〉 〈p〉4.4.1 Retention in NP Systems 186〈/p〉 〈p〉4.4.2 Solvent Strength in Liquid-Solid Chromatography 188〈/p〉 〈p〉4.4.3 Pilot Technique Thin-Layer Chromatography Using the PRISMA Model 190〈/p〉 〈p〉4.4.3.1 Step (1): Solvent Strength Adjustment 199〈/p〉 〈p〉4.4.3.2 Step (2): Optimization of Selectivity 199〈/p〉 〈p〉4.4.3.3 Step (3): Final Optimization of the Solvent Strength 200〈/p〉 〈p〉4.4.3.4 Step (4): Determination of the Optimum Mobile Phase Composition 200〈/p〉 〈p〉4.4.4 Strategy for an Industrial Preparative Chromatography Laboratory 202〈/p〉 〈p〉4.4.4.1 Standard Gradient Elution Method on Silica 203〈/p〉 〈p〉4.4.4.2 Simplified Procedure 204〈/p〉 〈p〉4.5 Criteria for Choosing Reversed Phase Systems 206〈/p〉 〈p〉4.5.1 Retention and Selectivity in RP Systems 208〈/p〉 〈p〉4.5.2 Gradient Elution for Small Amounts of Product on RP Columns 212〈/p〉 〈p〉4.5.3 Rigorous Optimization for Isocratic Runs 213〈/p〉 〈p〉4.5.4 Rigorous Optimization for Gradient Runs 217〈/p〉 〈p〉4.5.5 Practical Recommendations 222〈/p〉 〈p〉4.6 Criteria for Choosing CSP Systems 223〈/p〉 〈p〉4.6.1 Suitability of Preparative CSP 223〈/p〉 〈p〉4.6.2 Development of Enantioselectivity 224〈/p〉 〈p〉4.6.3 Optimization of Separation Conditions 226〈/p〉 〈p〉4.6.3.1 Determination of Racemate Solubility 226〈/p〉 〈p〉4.6.3.2 Selection of Elution Order 226〈/p〉 〈p〉4.6.3.3 Optimization of Mobile/Stationary Phase Composition, Including Temperature 226〈/p〉 〈p〉4.6.3.4 Determination of Optimum Separation Step 227〈/p〉 〈p〉4.6.4 Practical Recommendations 227〈/p〉 〈p〉4.7 Downstream Processing of mAbs Using Protein A and IEX 231〈/p〉 〈p〉4.8 Size-Exclusion Chromatography (SEC) 236〈/p〉 〈p〉4.9 Overall Chromatographic System Optimization 237〈/p〉 〈p〉4.9.1 Conflicts During Optimization of Chromatographic Systems 237〈/p〉 〈p〉4.9.2 Stationary Phase Gradients 241〈/p〉 〈p〉References 246〈/p〉 〈p〉〈b〉5 Process Concepts 〈/b〉〈b〉251〈br /〉〈/b〉〈i〉Malte Kaspereit and Henner Schmidt-Traub〈/i〉〈/p〉 〈p〉5.1 Discontinuous Processes 252〈/p〉 〈p〉5.1.1 Isocratic Operation 252〈/p〉 〈p〉5.1.2 Gradient Chromatography 253〈/p〉 〈p〉5.1.3 Closed-Loop Recycling Chromatography 256〈/p〉 〈p〉5.1.4 Steady-State Recycling Chromatography (SSRC) 258〈/p〉 〈p〉5.1.5 Flip-Flop Chromatography 259〈/p&g
    Language: English
    Keywords: Electronic books. ; Electronic books. ; Electronic books.
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/9783527816347
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/9783527816347
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/9783527816347
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  • 5
    Book
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    Mathematische Modellierung der präparativen Flüssigchromatographie (1994)
    Details
    UID:
    b3kat_BV024404902
    Format: 172 S. , graph. Darst.
    Note: Berlin, Techn. Univ., Habil.-Schr., 1995
    Language: Undetermined
    Keywords: Flüssigkeitschromatographie ; Trennverfahren ; Mathematisches Modell ; Hochschulschrift
    Author information: Seidel-Morgenstern, Andreas 1956-
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  • 6
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    Mathematische Modellierung der präparativen Flüssigchromatographie (1995)
    Wiesbaden : DUV, Dt. Univ.-Verl.
    Details
    UID:
    b3kat_BV023760706
    Format: 187 S. , graph. Darst.
    ISBN: 3824420643
    Series Statement: DUV : Naturwissenschaft
    Note: Zugl.: Berlin, Techn. Univ., Habil.-Schr., 1995
    Language: German
    Keywords: Flüssigkeitschromatographie ; Trennverfahren ; Mathematisches Modell ; Hochschulschrift
    Author information: Seidel-Morgenstern, Andreas 1956-
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  • 7
    Online Resource
    Online Resource
    Preparative chromatography (2020)
    Weinheim : Wiley-VCH
    Details
    UID:
    b3kat_BV046901661
    Format: 1 Online-Ressource (xxviii, 620 Seiten)
    Edition: Third edition
    ISBN: 9783527816330 , 9783527816347 , 9783527816316
    Additional Edition: Erscheint auch als Druck-Ausgabe ISBN 978-3-527-34486-4
    Language: English
    Subjects: Chemistry/Pharmacy
    RVK:
    VG 7200
    Keywords: Präparative Chromatographie ; Chromatographie ; Aufsatzsammlung
    DOI: 10.1002/9783527816347
    URL: Volltext  (URL des Erstveröffentlichers)
    Author information: Schmidt-Traub, Henner 1940-2020
    Author information: Seidel-Morgenstern, Andreas 1956-
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  • 8
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    Book
    Enantiomerentrennung mit molekular geprägten, monolithischen Polymerphasen (2012)
    Barleben : docupoint Verlag
    Details
    UID:
    b3kat_BV046625515
    Format: XII, 183 Seiten , graph. Darst , 21 cm
    ISBN: 9783869120690
    Note: Dissertation Universität Magdeburg 2011
    Language: German
    Keywords: Polymere ; Molekulares Prägen ; Enantiomerentrennung ; HPLC ; Stationäre Phase ; Membranverfahren ; Hochschulschrift
    URL: Inhaltsverzeichnis
    Author information: Scheffler, Franziska 1964-
    Author information: Seidel-Morgenstern, Andreas 1956-
    Author information: Seebach, Axel 1967-
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  • 9
    Online Resource
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    Preparative chromatography / (2012)
    Weinheim :Wiley,
    Details
    UID:
    almafu_9959328924202883
    Format: 1 online resource (806 pages)
    Edition: 2nd completely rev. and updated ed.
    ISBN: 9783527649310 , 352764931X , 9781283714426 , 1283714426 , 9783527649280 , 352764928X
    Content: Completely revised to reflect the developments in this fast-changing field, this new edition features 35 % new content. It retains the interdisciplinary approach that elegantly combines the chemistry and engineering involved to describe the conception and improvement of chromatographic processes. It also covers recent advances in preparative chromatographic processes for the separation of "smaller" molecules using standard laboratory equipment as well as the detailed conception of industrial chemical plants. The increase in biopharmaceutical substances is reflected by new and revised chapters.
    Note: Introduction / Henner Schmidt-Traub, Reinhard Ditz -- Fundamentals and general terminology / Andreas Seidel-Morgenstern, Michael Schulte, Achim Epping -- Stationary phases and chromatographic systems / Michael Schulte, Matthias Jöhnck, Romas Skudas, Klaus K Unger, Cedric du Fresne von Hohenesche, Wolfgang Wewers, Jules Dingenen, Joachim Kinkel -- Chromatography equipment: engineering and operation / Abdelaziz Toumi, Jules Dingenen, Joel Genolet, Olivier Ludemann-Hombourger, Andre Kiesewetter, Martin Krahe, Michele Morelli, Henner Schmidt-Traub, Andreas Stein, Eric Valery -- Process concepts / Malte Kaspereit, Michael Schulte, Klaus Wekenborg, Wolfgang Wewers -- Modeling and model parameters / Andreas Seidel-Morgenstern, Henner Schmidt-Traub, Mirko Michel, Achim Epping, Andreas Jupke -- Model-based design, optimization, and control / Henner Schmidt-Traub, Malte Kaspereit, Sebastian Engell, Arthur Susanto, Achim Epping, Andreas Jupke -- Appendix A: data of test systems -- Index.
    Language: English
    Keywords: Electronic books. ; Electronic books.
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/9783527649280
    URL: https://onlinelibrary.wiley.com/doi/book/10.1002/9783527649280
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  • 10
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    Mandelic acid single-crystal growth : experiments VS numerical simulations (2023)
    Show associated volumes
    Details
    UID:
    gbv_1870742257
    ISSN: 1991-7120
    In: Communications in computational physics, Hong Kong : Global Science Press, 2006, 33(2023), 1, Seite 77-100, 1991-7120
    In: volume:33
    In: year:2023
    In: number:1
    In: pages:77-100
    Language: English
    DOI: 10.4208/cicp.oa-2022-0035
    URL: https://doi.org/10.4208/cicp.oa-2022-0035
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