In:
Journal of AOAC INTERNATIONAL, Oxford University Press (OUP), Vol. 63, No. 1 ( 1980-01-01), p. 47-48
Abstract:
A high performance liquid chromotographic method is presented for determining bendiocarb (2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate) on wool. Bendiocarb is extracted from wool with methanol containing methyl benzoate as internal standard, eluted through a Zorbax ODS column with methanol-water (55 + 45), and detected with a UV detector at 280 nm. The method can be used to determine bendiocarb at 0.001–0.02% by weight. The limit of detection is 0.0004%, or 4 ppm. At 4 analyses each, recovery at 0.013% was 101%, standard deviation 2.8%; at 0.003%, recovery was 96%, standard deviation 5.6%; at 0.001%, recovery was 103%, standard deviation 2.9%.
Type of Medium:
Online Resource
ISSN:
0004-5756
DOI:
10.1093/jaoac/63.1.47
Language:
English
Publisher:
Oxford University Press (OUP)
Publication Date:
1980
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