UID:
almafu_9958126642502883
Umfang:
1 online resource (668 p.)
Ausgabe:
2nd ed.
ISBN:
0-08-091699-6
Inhalt:
Nuclear Magnetic Resonance Spectroscopy
Anmerkung:
"Published by arrangement with AT&T."
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Front Cover; Nuclear Magnetic Resonance Spectroscopy; Copyright Page; Table of Contents; Foreword; Preface to the First Edition; Preface to the Second Edition; Chapter 1. Fundamental Principles; 1.1 Introduction; 1.2 Nuclear Spin; 1.3 The Nuclear Magnetic Resonance Phenomenon; 1.4 The Detection of the Resonance Phenomenon: CW and Pulse Fourier Transform Methods; 1.5 Spin-Lattice Relaxation; 1.6 Dipolar Broadening and Spin-Spin Relaxation; 1.7 The Bloch Equations; 1.8 Saturation; 1.9 Nuclear Electric Quadrupole Relaxation; 1.10 Magnetic Shielding and Chemical Shift
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1.11 Electron-Mediated Coupling of Nuclear SpinsReferences; Chapter 2. Experimental Methods; 2.1 Introduction; 2.2 Overview of the NMR Experiment; 2.3 The Magnetic Field; 2.4 Causing Transitions between the Nuclear Energy Levels; 2.5 Detecting the Signal; 2.6 Processing and Presenting the Data; 2.7 Preparing the Sample; 2.8 Resolution and Sensitivity Considerations; References; Chapter 3. The Chemical Shift; 3.1 Introduction; 3.2 Atomic Shielding; 3.3 Molecular Shielding; References; Chapter 4. Coupling of Nuclear Spins; 4.1 Introduction; 4.2 Description and Analysis of Spin Systems
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4.3 Dependence of J Coupling on Structure and Geometry4.4 Spin Decoupling and Associated Techniques; References; Chapter 5. Nuclear Relaxation and Chemical Rate Processes; 5.1 Introduction; 5.2 Spin Lattice Relaxation; 5.3 Spin-Spin Relaxation; 5.4 Rate Processes; References; Chapter 6. Two-Dimensional Nuclear Magnetic Resonance Spectroscopy; 6.1 Introduction; 6.2 J-Resolved Spectroscopy; 6.3 Correlated Spectroscopy; 6.4 Multiple Quantum Spectroscopy; References; Chapter 7. Macromolecules; 7.1 Introduction; 7.2 Chain Microstructure; 7.3 Biopolymers; 7.4 Chain Motion in Macromolecules
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ReferencesChapter 8. NMR of Solids; 8.1 Introduction; 8.2 Proton Dipolar Broadening; 8.3 Chemical Shift Anisotropy; 8.4 Magic Angle Spinning; 8.5 Cross Polarization; 8.6 Magic Angle Spectra; 8.7 Multiple-Pulse Line Narrowing; 8.8 Deuterium Quadruple Echo NMR; References; Chapter 9. Special Topics; 9.1 Less Common Nuclei; 9.2 NMR Imaging; 9.3 Solvent Suppression; 9.4 Zero Field NMR; References; Appendix A: Table of Nuclear Properties; Appendix B: Calculated Proton Spectra; Appendix C: Proton Spin-Spin Coupling Constants; Appendix D: Carbon-Proton Spin-Spin Coupling Constants; Author Index
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Subject Index
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English
Weitere Ausg.:
ISBN 0-12-119752-2
Sprache:
Englisch
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