UID:
almafu_9960073342802883
Format:
1 online resource (335 p.)
ISBN:
1-281-77860-5
,
9786611778606
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0-08-085839-2
Series Statement:
Journal of chromatography library ; v. 36
Content:
This book gives a comprehensive, up-to-date review of all selective detectors used in combination with gas chromatography. For each detector, the historical background, design and principle are described, and the working parameters affecting the detector performance are analyzed critically and in detail. The analytical possibilities of the detectors and the main characteristics such as sensitivity, noise and minimum detectability are discussed. All the selective detectors that are currently used are discussed in detail. Combinations of GC with other techniques such as plasma emission spectros
Note:
Description based upon print version of record.
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Front Cover; Selective Gas Chromatographic Detectors; Copyright Page; Contents; Journal of Chromatography Library (other volumes in the series); Preface; Chapter 1. Introduction; References; Chapter 2. Basic terms relating to detectors; 2.1. Detector sensitivity; 2.2. Minimum detectability; 2.3. Detection limit; 2.4. Detector noise; 2.5. Dependence of detector response on amount of compound; 2.6. Selectivity of response; References; Chapter 3. Alkali flame - ionization detector; 3.1. Introduction; 3.2. Detector design; 3.3. Detector life, reproducibility of response
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3.4. Background current (hydrogen flow-rate)3.5. Negative response; 3.6. Response to individual heteroatoms; 3.7. Influence of compound structure on detector response; 3.8. Influence of main operational parameters on detector response; 3.9. Detection mechanism; References; Chapter 4. Flameless alkali sensitized detectors; 4.1. Introduction; 4.2. The Perkin-Elmer detector; 4.3. The Hewlett-Packard detector; 4.4. The Tracor detector; 4.5. The Varian detector; 4.6. The Detector Engineering Technology detector; 4.7. The chemi - ionization detector
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4.8. Detector life and reproducibility of response4.9. Detectors for halogen compounds; References; Chapter 5. Flame-ionization detector; 5.1. Introduction; 5.2. Hydrogen atmosphere flame-ionization detector; 5.3. Hydrogen atmosphere flame-ionization detector for silicon compounds; 5.4. Flame-ionization detector with hydrocarbon background; 5.5. Selective detection of halogen compounds; References; Chapter 6. Photoionization detector; 6.1. Introduction; 6.2. Response model; 6.3. Sensitivity of response and minimum detectability; 6.4. Selectivity of response; 6.5. Carrier gas; References
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Chapter 7. Flame photometric detector7.1. Introduction; 7.2. Response model; 7.3. Detector sensitivity and minimum detectability; 7.4. Selectivity of response; 7.5. Tin and germanium compounds; 7.6. Halogen compounds; 7.7. Other detection possibilities; 7.8. Linearity of response; 7.9. Sulphur background; 7.10. Response quenching; 7.11. Flame stability; 7.12. Other identification possibilities; References; Chapter 8. Chemiluminescence detectors; 8.1. Introduction; 8.2. Detector for N-nitroso compounds; 8.3. Detector for nitroaromatic compounds; 8.4. Detector for nitrogen-containing compounds
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8.5. Ozone chemiluminescence detector for compounds not containing nitrogen8.5A. Redox chemiluminescence detector; 8.6. Chemiluminescence detector with sodium metal; 8.7. Fluorine-induced detector; References; Chapter 9. Electrolytic conductivity detector; 9.1. Detector construction; 9.2. Selectivity of response; 9.3. Response; 9.4. Solvent; 9.5. Gases; 9.6. Temperature; References; Chapter 10. Coulometric detector; 10.1. Introduction; 10.2. Response; 10.3. Quantitative results; References; Chapter 11. Electron-capture detector; 11.1. Introduction; 11.2. Design
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11.3. Sources of primary electrons
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English
Additional Edition:
ISBN 0-444-42488-1
Language:
English
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