In:
Powder Diffraction, Cambridge University Press (CUP), Vol. 3, No. 2 ( 1988-06), p. 78-80
Abstract:
A nonlinear optical material 4-(N,N-dimethylamino)-3-acetamidonitrobenzene, (CH 3 ) 2 NC 6 H 3 NO 2 NHCOCH 3 , has been characterized by X-ray powder diffractometer method. The experimental 2 θ values corrected for systematic errors, the relative intensities, values of d exp and the Miller indices of the 46 peaks observed in the 5° to 51° 2 θ range are reported. The powder diffraction data have been evaluated, and the figure of merit is F 30 = 36.6 (0.016, 51). The unit cell parameter least-squares refined from 38 non-overlapping peaks of the monoclinic compound with a P2 1 space group are: a = 4.792(1)Å, b = 13.055(2)Å, c = 8.735(1)Å, β = 94.43(2)°, V = 544.8(1)Å 3 , Z = 2, and D x = 1.36 gm/cm 3 . The powder diffraction results are in a good agreement with those obtained from single-crystal structure data.
Type of Medium:
Online Resource
ISSN:
0885-7156
,
1945-7413
DOI:
10.1017/S0885715600013269
Language:
English
Publisher:
Cambridge University Press (CUP)
Publication Date:
1988
detail.hit.zdb_id:
2047596-2