In:
Applied Mechanics and Materials, Trans Tech Publications, Ltd., Vol. 577 ( 2014-7), p. 7-10
Abstract:
In this paper, the prenyl alcohol was catalyzed synthesized by using isoprene and dichloroacetic acid as raw material and sodium dichloroacetate as catalyst. The obtained product was mainly characterized by FT-IR and GC. Furthermore, the olefine acid ratio, reaction time, amount of catalyst, saponification time, NaOH concentration and distilled water consumption were systematically investigated during the work. The optimum reaction conditions were as follows: the olefine acid ratio was 1:2, reaction time was 2h, amount of catalyst was 1.5g, saponification time was 2h, NaOH concentration was 4mol/L and amount of distilled water was 0.2mL, the yield of prenyl alcohol was 26%
Type of Medium:
Online Resource
ISSN:
1662-7482
DOI:
10.4028/www.scientific.net/AMM.577
DOI:
10.4028/www.scientific.net/AMM.577.7
Language:
Unknown
Publisher:
Trans Tech Publications, Ltd.
Publication Date:
2014
detail.hit.zdb_id:
2251882-4