In:
Advanced Materials Research, Trans Tech Publications, Ltd., Vol. 304 ( 2011-7), p. 119-123
Kurzfassung:
We report herein synthesis and characterization of CuInS 2 and CuInSe 2 compounds by vacuum sintering method. In this study, the manual-milled and ball-milled precursors including copper, indium, and sulfur (selenium) elements were sintered under vacuum at different temperatures for synthesis of CuInS 2 and CuInSe 2 compounds, respectively. The crystal structure, morphology and Raman property of the sintered powder were investigated by X-ray diffraction, scanning electron microscope and Raman scattering spectroscopy, respectively. The results show that the structure of the products, which was sintered with the manual-milled and ball-milled precursors, were transformed into the single chalcopyrite phase CuInS 2 powder at 923K and 623K, and the grain size are about 2~3μm and 250 nm, respectively. In addition, the CuInSe2 powder was synthesized about 723K via using the ball-milled powder including copper, indium, and selenium elements as the precursor.
Materialart:
Online-Ressource
ISSN:
1662-8985
DOI:
10.4028/www.scientific.net/AMR.304
DOI:
10.4028/www.scientific.net/AMR.304.119
Sprache:
Unbekannt
Verlag:
Trans Tech Publications, Ltd.
Publikationsdatum:
2011
ZDB Id:
2265002-7